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ChemicalBook CAS DataBase List O-Bis(2-aMinoethoxy)benzene
42988-85-2

O-Bis(2-aMinoethoxy)benzene synthesis

4synthesis methods
27165-64-6 Synthesis
1,2-Phenylenedioxydiacetonitrile

27165-64-6
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Yield:42988-85-2 76 %

Reaction Conditions:

Stage #1: 1,2-Di(cyanomethoxy)-benzolwith dimethylsulfide borane complex in tetrahydrofuran;Inert atmosphere;Reflux;
Stage #2: with hydrogenchloride in water;Reflux;

References:

WO2022/251496,2022,A1 Location in patent:Paragraph 0139; 0153; 0156; 0157

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