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25392-50-1

Oxazorone synthesis

4synthesis methods
-

Yield:25392-50-1 99%

Reaction Conditions:

in 2-methoxy-ethanol; for 6 h;Reflux;

Steps:

21.21-2

Step 21-2: Compound 21-A (410 mg, 2.35 mmol) was dissolved in 2-methoxyethanol,Morpholine (410 mg, 4.7 mmol) was added and refluxed for 6 h. After the reaction is complete, concentrate,Column chromatography gave compound 21-B (610 mg, 99%) as a yellow solid.

References:

CN114315733,2022,A Location in patent:Paragraph 0140-0141; 0143