oxonan-2-one synthesis

9synthesis methods

Product Name:oxonan-2-one
CAS Number:5698-29-3
Molecular formula:C8H14O2
Molecular Weight:142.2

502-49-8 Synthesis

502-49-8
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5698-29-3
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Yield:5698-29-3 88%

Reaction Conditions:

with Ag/WO₃ nanobars;dihydrogen peroxide in acetonitrile at 80; for 9 h;Green chemistry;Baeyer-Villiger Ketone Oxidation;

Steps:

2.2. Reaction setup
General procedure: Liquid phase oxidation reaction was carried out in a two-neck round bottom flask. The reaction temperature was ranged between RT and 100 °C. Small aliquots of the sample were withdrawn from the reaction mixture at regular intervals for analysis using a syringe. At the end of the reaction, the catalyst was separated by filtration and the products were analyzed by GC (FID) and GCMS

References:

Ghosh, Shilpi;Acharyya, Shankha Shubhra;Singh, Raghuvir;Gupta, Piyush;Bal, Rajaram [Catalysis Communications,2015,vol. 72,p. 33 - 37]

FullText

17696-11-6 Synthesis