p-nitrophenyl dimethylsulphamate synthesis
2synthesis methods
- Product Name:p-nitrophenyl dimethylsulphamate
- CAS Number:1142-27-4
- Molecular formula:C8H10N2O5S
- Molecular Weight:246.2404
Yield:1142-27-4 90%
Reaction Conditions:
Stage #1: 4-nitro-phenolwith dmap;triethylamine in dichloromethane at 20; for 0.166667 h;
Stage #2: dimethylamino sulfonyl chloride in dichloromethane at 20; for 16 h;
References:
Molander, Gary A.;Shin, Inji [Organic Letters,2013,vol. 15,# 10,p. 2534 - 2537] Location in patent:supporting information
