PENTAFLUOROPROPIONALDEHYDE METHYL HEMIACETAL synthesis
- Product Name:PENTAFLUOROPROPIONALDEHYDE METHYL HEMIACETAL
- CAS Number:59872-84-3
- Molecular formula:C4H5F5O2
- Molecular Weight:180.07
378-75-6
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Yield:59872-84-3 73 %Spectr.
Reaction Conditions:
Stage #1: perfluoropropionic acid methyl esterwith dichloro(triphenylphosphine){2-diphenylphosphino-N-[2-(methylthio)ethyl]ethylamine}ruthenium(II);potassium tert-butylate in methanol;Inert atmosphere;Glovebox;
Stage #2: with hydrogen in methanol at 40; under 18751.9 Torr; for 24 h;Catalytic behavior;Autoclave;Sealed tube;Reagent/catalyst;
References:
Dub, Pavel A.;Batrice, Rami J.;Gordon, John C.;Scott, Brian L.;Minko, Yury;Schmidt, Jurgen G.;Williams, Robert F. [Organic Process Research and Development,2020,vol. 24,# 3,p. 415 - 442]
