Phenanthrene, 3-chloro-9-phenyl- synthesis
- Product Name:Phenanthrene, 3-chloro-9-phenyl-
- CAS Number:94546-54-0
- Molecular formula:C20H13Cl
- Molecular Weight:288.77
Yield:94546-54-0 61%
Reaction Conditions:
with palladium diacetate;potassium carbonate;bis[2-(diphenylphosphino)phenyl] ether in 1,4-dioxane at 130; for 5 h;Inert atmosphere;Schlenk technique;Sealed tube;regioselective reaction;
References:
Wei, Dong;Li, Meng-Yao;Zhu, Bin-Bin;Yang, Xiao-Di;Zhang, Fang;Feng, Chen-Guo;Lin, Guo-Qiang [Angewandte Chemie - International Edition,2019,vol. 58,# 46,p. 16543 - 16547][Angew. Chem.,2019,vol. 131,# 46,p. 16695 - 16699,5] Location in patent:supporting information
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