Propane, 2-diazo-1,1,1,3,3,3-hexafluoro- synthesis
- Product Name:Propane, 2-diazo-1,1,1,3,3,3-hexafluoro-
- CAS Number:684-23-1
- Molecular formula:C3F6N2
- Molecular Weight:178.0359
1588-41-6
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684-23-1
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Yield:684-23-1 76-79
Reaction Conditions:
with lead(IV) acetate in benzonitrile;addn. of (CF3)2CNNH2 soln. in C6H5CN to suspension of Pb(CH3COO)4 in C6H5CN, mixing at 0°C under N2, warming to 20°C, mixing (1 h);
References:
Gale,D.M. et al. [Journal of the American Chemical Society,1966,vol. 88,p. 3617 - 3623] Middleton, W. J.;Gale, D. M. [Organic Syntheses,1970,vol. 50,p. 6 - 9]
1619-92-7
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$25.00/250mg
684-23-1
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3024-50-8
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684-23-1
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2154-71-4
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1588-41-6
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359-63-7
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684-23-1
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