Propanoic acid, 3-(3,5-dimethylphenoxy)- synthesis
- Product Name:Propanoic acid, 3-(3,5-dimethylphenoxy)-
- CAS Number:7507-34-8
- Molecular formula:C11H14O3
- Molecular Weight:194.23
3649-02-3
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Yield:7507-34-8 92%
Reaction Conditions:
with hydrogenchloride in water at 80 - 90;
Steps:
General experimental procedure for the synthesis of 3-aryloxypropanoic acids (3a-3o)
General procedure: Mixture of 3-aryloxypropane nitrile (2a-2o) (2 mmol) and conc. HCl (1-2 mL) is heated at 80-90 °C for about 1- 2 h (after monitoring the reaction completion by TLC). Cooled the reaction mass and added ice water to obtain solid 3-aryloxypropanoic acid (3a-3o) as solids which is filtered and dried to be taken up for the subsequent step.
References:
Begum, Ayisha F.;Balasubramanian, Kalpattu K.;Shanmugasundaram, Bhagavathy [Tetrahedron Letters,2021,vol. 82,art. no. 153372] Location in patent:supporting information
108-68-9
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