PSI7409 synthesis
- Product Name:PSI7409
- CAS Number:1015073-42-3
- Molecular formula:C10H16FN2O14P3
- Molecular Weight:500.16
58-96-8
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1015073-42-3
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Yield:-
Steps:
Multi-step reaction with 9 steps
1.1: pyridine / 16 h / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 16 h / 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran
4.1: triethylamine hydrofluoride / tetrahydrofuran
5.1: pyridine
6.1: diethylamino-sulfur trifluoride / dichloromethane
7.1: ammonia / methanol
8.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trimethyl phosphite / tetrahydrofuran / 0.17 h / 20 °C / Sonication; Inert atmosphere
8.2: 1 h / 20 °C / Inert atmosphere
9.1: bis(tri-n-butylammonium) pyrophosphate; tributyl-amine / N,N-dimethyl-formamide / 0.08 h / 20 °C
References:
Wang, Gang;Lim, Siew Pheng;Chen, Yen-Liang;Hunziker, Jürg;Rao, Ranga;Gu, Feng;Seh, Cheah Chen;Ghafar, Nahdiyah Abdul;Xu, Haoying;Chan, Katherine;Lin, Xiaodong;Saunders, Oliver L.;Fenaux, Martijn;Zhong, Weidong;Shi, Pei-Yong;Yokokawa, Fumiaki [Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,# 13,p. 2324 - 2327]
1015073-43-4
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1015073-42-3
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863329-66-2
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1015073-42-3
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114262-45-2
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1015073-42-3
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114262-49-6
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1015073-42-3
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