(R)-ACETYLAMINO-CYCLOHEXYL-ACETIC ACID synthesis
- Product Name:(R)-ACETYLAMINO-CYCLOHEXYL-ACETIC ACID
- CAS Number:14429-43-7
- Molecular formula:C10H17NO3
- Molecular Weight:199.25
167424-24-0
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Yield:14429-43-7 75%
Reaction Conditions:
with hydrogen;platinum(IV) oxide in methanol; for 4 h;
Steps:
4
To a solution of 15g of (R)-(acetylamino)(1,4-cyclohexadiene-l-yl)acetic acid in SOOmL of methanol was added SOOmg of platinum oxide, and the mixture was stirred for 4 hours under hydrogen gas atmosphere. Then, the reaction mixture was filtrated and the filtrate was condensed. The residue was recrystallized from ethanol to give 11.4g (75%) of the title compound.
References:
WO2004/111053,2004,A1 Location in patent:Page/Page column 20
60-35-5
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201230-82-2
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2043-61-0
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78781-84-7
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5664-29-9
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$8.00/250mg
108-24-7
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