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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
882424-02-4

(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL synthesis

5synthesis methods
Ethyl 4,4,4-trifluorocrotonate

25597-16-4
231 suppliers
$7.00/1g

(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL

882424-02-4
6 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 92 percent / Br2 / CCl4 / 5 h / Heating
2: ethanol / 18 h / -5 - 20 °C
3: MgBr2, H2SO4 / tetrahydrofuran / 0.17 h / -10 °C
4: H2, AcOH / 10 percent Pd/C / ethyl acetate / 16 h / 760 Torr / Ambient temperature

References:

Davoli, Paolo;Forni, Arrigo;Franciosi, Chiara;Moretti, Irene;Prati, Fabio [Tetrahedron Asymmetry,1999,vol. 10,# 12,p. 2361 - 2371]

Butanoic acid, 4,4,4-trifluoro-3-[[(1R)-2-hydroxy-1-phenylethyl]amino]-, ethyl ester, (3R)-

461440-80-2
0 suppliers
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(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL

882424-02-4
6 suppliers
inquiry

References
Butanoic acid, 2,3-dibromo-4,4,4-trifluoro-, ethyl ester

363-57-5
0 suppliers
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(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL

882424-02-4
6 suppliers
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References
ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTYRATE

170804-18-9
65 suppliers
$42.79/250mg

(S)-3-Amino-4,4,4-trifluoro-butyric acid ethyl ester

885220-93-9
1 suppliers
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(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL

882424-02-4
6 suppliers
inquiry

References
372-31-6 Synthesis
Ethyl 4,4,4-trifluoroacetoacetate

372-31-6
482 suppliers
$5.00/10g

(R)-ETHYL 3-AMINO-4,4,4-TRIFLUOROBUTANOATE HCL

882424-02-4
6 suppliers
inquiry

References