(S)-8-tert-butylchroman-4-amine synthesis
- Product Name:(S)-8-tert-butylchroman-4-amine
- CAS Number:1228553-77-2
- Molecular formula:C13H19NO
- Molecular Weight:205.3
88-18-6
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: potassium carbonate / acetonitrile / 96 h / 20 °C
2: N-chloro-succinimide; silver(I) acetate / acetone / 4 h / Reflux
3: ethylene glycol / 4 h / Reflux
4: pyridine / 24 h / 20 °C
5: palladium 10% on activated carbon; ammonia; hydrogen / methanol / 1 h / 20 °C / 3102.97 Torr
References:
Schmidt, Robert G.;Bayburt, Erol K.;Latshaw, Steven P.;Koenig, John R.;Daanen, Jerome F.;McDonald, Heath A.;Bianchi, Bruce R.;Zhong, Chengmin;Joshi, Shailen;Honore, Prisca;Marsh, Kennan C.;Lee, Chih-Hung;Faltynek, Connie R.;Gomtsyan, Arthur [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 5,p. 1338 - 1341]
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