salireposide synthesis
- Product Name:salireposide
- CAS Number:16955-55-8
- Molecular formula:C20H22O9
- Molecular Weight:406.38
![2-[(Benzoyloxy)methyl]-4-acetyloxyphenyl 2-O,3-O,4-O,6-O-tetraacetyl-β-D-glucopyranoside](/CAS/20180808/GIF/18265-35-5.gif)
18265-35-5
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16955-55-8
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Yield:16955-55-8 71%
Reaction Conditions:
with hydrogenchloride in ethanol;chloroform;water at 20; for 48 h;
Steps:
5
General procedure: To a glycoside (14, 15, 17-19) (0.15 mmol) in a mixture of 96%- ethanol and CHCl3 in proportion 1.5-0.5 mL was added 0.5 mL 36% HCl. The reaction mixture was stirred and then kept at room temperature for a 24-48 h. The reaction mixture was neutralized with 20%-solution of Na2CO3 until pH 7, evaporated to dryness and product was isolated employing column chromatography by gradient elution using chloroform and chloroform-ethanol mixture (from ratio 9:1 to 4:1). Analytical samples were purified by recrystallization from ethanol.
References:
Belyanin, Maxim L.;Stepanova, Elena V.;Ogorodnikov, Vladimir D. [Carbohydrate Research,2012,vol. 363,p. 66 - 72]
123-31-9
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$13.00/25g
16955-55-8
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64418-88-8
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16955-55-8
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3233-32-7
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$27.00/1g
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