sodium (Z)-octadec-9-enyl sulphate synthesis
- Product Name:sodium (Z)-octadec-9-enyl sulphate
- CAS Number:1847-55-8
- Molecular formula:C18H37NaO4S
- Molecular Weight:372.54
112-62-9
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 90 percent / LiAlH4 / diethyl ether
2: 1) SO3*Me3N, 2) a) 3 M aq. NaOH, b) Biorad AG 50W-X4 (Na(+) form) ion-exchange resin / 1) 125 deg C, 6 h, 2) a) to pH 10, b) MeOH, 25 deg C, 4 h
References:
Jaeger, David A.;Sayed, Yasmin M. [Journal of Organic Chemistry,1993,vol. 58,# 9,p. 2619 - 2627]
143-28-2
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