ChemicalBook CAS DataBase List STAUROSPORINE

STAUROSPORINE synthesis

2synthesis methods

Product Name:STAUROSPORINE
CAS Number:62996-74-1
Molecular formula:C28H26N4O3
Molecular Weight:466.54

9,13-Epoxy-1H,11H-diindolo[1,2,3-gh:3',2',1'-lm]pyrrolo[3,4-j][1,7]benzodiazonine-1,11-dione, 2-[(3,4-dimethoxyphenyl)methyl]-2,3,9,10,12,13-hexahydro-10-methoxy-9-methyl-, 11-(O-methyloxime), [9S-(9α,10β,11Z,13α)]- (9CI)

195617-12-0
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62996-74-1
355 suppliers
$28.00/500μg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 79 mg / H₂ / PtO₂ / aq. acetic acid
2: 2.) BH₃*DMS / 1) THF; 2) THF, toluene, reflux, 2 h
3: 70 percent / TFA, anisole / 48 h

References:

Wood, John L.;Stoltz, Brian M.;Goodman, Steven N.;Onwueme, Kenolisa [Journal of the American Chemical Society,1997,vol. 119,# 41,p. 9652 - 9661]

9,13-Epoxy-1H,9H-diindolo[1,2,3-gh:3',2',1'-lm]pyrrolo[3,4-j][1,7]benzodiazonin-1-one, 2-[(3,4-dimethoxyphenyl)methyl]-2,3,10,11,12,13-hexahydro-10-methoxy-9-methyl-11-(methylamino)-, [9S-(9α,10β,11β,13α)]- (9CI)

188028-33-3
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62996-74-1
355 suppliers
$28.00/500μg

References

STAUROSPORINE Related Search:

Diphenhydramine Hydrochloride Methimazole Succinylcholine Chloride K-252C

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