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443295-32-7

tert-butyl 1,2-diazepane-1-carboxylate synthesis

3synthesis methods
1-Benzyl 2-(tert-butyl) 1,2-diazepane-1,2-dicarboxylate

443295-19-0
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tert-butyl 1,2-diazepane-1-carboxylate

443295-32-7
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Yield:443295-32-7 96%

Reaction Conditions:

with hydrogen;palladium on activated charcoal in methanol at 20; under 760 Torr; for 3 h;

References:

Toya, Tetsuya;Yamaguchi, Kentaro;Endo, Yasuyuki [Bioorganic and Medicinal Chemistry,2002,vol. 10,# 4,p. 953 - 961]