tert-butyl 2-broMo-6-chloropyridin-3-ylcarbaMate synthesis
- Product Name:tert-butyl 2-broMo-6-chloropyridin-3-ylcarbaMate
- CAS Number:1227958-32-8
- Molecular formula:C10H12BrClN2O2
- Molecular Weight:307.57
5350-93-6
408 suppliers
$6.00/5g
1227958-32-8
68 suppliers
$45.00/10mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: N-Bromosuccinimide / N,N-dimethyl-formamide / 4 h / 15 - 25 °C / Inert atmosphere
2: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -5 - 20 °C / Inert atmosphere
References:
Grongsaard, Pintipa;Bulger, Paul G.;Wallace, Debra J.;Tan, Lushi;Chen, Qinghao;Dolman, Sarah J.;Nyrop, Jason;Hoerrner, R. Scott;Weisel, Mark;Arredondo, Juan;Itoh, Takahiro;Xie, Chengfu;Wen, Xianghui;Zhao, Dalian;Muzzio, Daniel J.;Bassan, Ephraim M.;Shultz, C. Scott [Organic Process Research and Development,2012,vol. 16,# 5,p. 1069 - 1081]
24424-99-5
811 suppliers
$13.50/25G
1050501-88-6
100 suppliers
$39.00/1g
1227958-32-8
68 suppliers
$45.00/10mg