tert-butyl(3R,5S)-5-fluoropiperidin-3-ylcarbamate synthesis
- Product Name:tert-butyl(3R,5S)-5-fluoropiperidin-3-ylcarbamate
- CAS Number:1363378-08-8
- Molecular formula:C10H19FN2O2
- Molecular Weight:218.27
24424-99-5
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1363378-08-8
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$45.00/2.5mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1,4-dioxane / 14 h / 20 °C / Inert atmosphere
2: diethylamino-sulfur trifluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
3: hydrogenchloride / water; ethanol / 1 h / 20 °C / Inert atmosphere
References:
Orliac, Aurelie;Routier, Julie;Burgat Charvillon, Fabienne;Sauer, Wolfgang H. B.;Bombrun, Agnes;Kulkarni, Santosh S.;Gomez Pardo, Domingo;Cossy, Janine [Chemistry - A European Journal,2014,vol. 20,# 13,p. 3813 - 3824]