tert-butyl 4-methoxy-2-nitrophenylcarbamate synthesis
- Product Name:tert-butyl 4-methoxy-2-nitrophenylcarbamate
- CAS Number:185428-90-4
- Molecular formula:C12H16N2O5
- Molecular Weight:268.27
Yield:185428-90-4 89%
Reaction Conditions:
Stage #1: 4-methoxy-2-nitroanilinewith sodium hydride in tetrahydrofuran;mineral oil; for 0.166667 h;
Stage #2: tert-butyldicarbonate in tetrahydrofuran;mineral oil at 20; for 24 h;
References:
Choi, Alex Wing-Tat;Yim, Vicki Man-Wai;Liu, Hua-Wei;Lo, Kenneth Kam-Wing [Chemistry - A European Journal,2014,vol. 20,# 31,p. 9633 - 9642] Location in patent:supporting information
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