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ChemicalBook CAS DataBase List tert-butyl 5-bromobenzo[d]thiazol-2-ylcarbamate
1160573-06-7

tert-butyl 5-bromobenzo[d]thiazol-2-ylcarbamate synthesis

6synthesis methods
20358-03-6 Synthesis
2-Amino-5-bromobenzothiazole

20358-03-6
149 suppliers
$8.00/250mg

tert-butyl 5-bromobenzo[d]thiazol-2-ylcarbamate

1160573-06-7
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Yield:1160573-06-7 94%

Steps:

274.1 Step 1:

Step 1:
tert-Butyl 5-bromobenzo[d]thiazol-2-ylcarbamate
The title compound (25.1 g, 94% yield) was generated from 5-bromobenzo[d]thiazol-2-amine (18.4 g, 80.3 mmol) following a procedure analogous to Example 214, step 1. LCMS (ESI): [M+H]+=329/331.

References:

US2018/65983,2018,A1

20358-03-6 Synthesis
2-Amino-5-bromobenzothiazole

20358-03-6
149 suppliers
$8.00/250mg

24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
867 suppliers
$13.50/25G

tert-butyl 5-bromobenzo[d]thiazol-2-ylcarbamate

1160573-06-7
8 suppliers
inquiry

93933-49-4 Synthesis
2-AMINO-4-BROMOBENZENETHIOL

93933-49-4
42 suppliers
inquiry

tert-butyl 5-bromobenzo[d]thiazol-2-ylcarbamate

1160573-06-7
8 suppliers
inquiry