tert-butyl 5-bromofuran-2-carboxylate synthesis
- Product Name:tert-butyl 5-bromofuran-2-carboxylate
- CAS Number:59862-83-8
- Molecular formula:C9H11BrO3
- Molecular Weight:247.09
32460-00-7
101 suppliers
$18.00/100mg
24424-99-5
860 suppliers
$13.50/25G
59862-83-8
21 suppliers
$552.25/1g
Yield:59862-83-8 84%
Reaction Conditions:
Stage #1: 2,5-dibromofuranwith n-butyllithium;butyl magnesium bromide in tetrahydrofuran;hexane;toluene at -10;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran;hexane;toluene at -10;
Stage #3: with citric acid in tetrahydrofuran;hexane;toluene;Further stages.;
References:
Li, Hongmei;Balsells, Jaume [Tetrahedron Letters,2008,vol. 49,# 12,p. 2034 - 2037]
585-70-6
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$10.15/1g
75-65-0
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$10.00/10ml
59862-83-8
21 suppliers
$552.25/1g
88-14-2
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$5.00/10g
59862-83-8
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$552.25/1g
26726-16-9
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$116.64/250mgs:
865-48-5
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$11.19/25G
59862-83-8
21 suppliers
$552.25/1g
585-70-6
222 suppliers
$10.15/1g
36805-97-7
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$29.00/1g
59862-83-8
21 suppliers
$552.25/1g