tert-butyl 5-methoxy-2-nitrophenylcarbamate synthesis
- Product Name:tert-butyl 5-methoxy-2-nitrophenylcarbamate
- CAS Number:185428-55-1
- Molecular formula:C12H16N2O5
- Molecular Weight:268.27
24424-99-5
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16133-49-6
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185428-55-1
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Yield:185428-55-1 92%
Reaction Conditions:
Stage #1: 5-methoxy-2-nitroanilinewith sodium hydride in tetrahydrofuran at 0 - 20; for 1.16667 h;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran at 20; for 2 h;
References:
EP1172356,2002,A1 Location in patent:Page 8
60144-52-7
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877671-39-1
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158461-29-1
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185428-55-1
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