TETRACHLOROBIS(TETRAHYDROFURAN)NIOBIUM(IV) synthesis
- Product Name:TETRACHLOROBIS(TETRAHYDROFURAN)NIOBIUM(IV)
- CAS Number:61247-57-2
- Molecular formula:C4H8Cl4NbO
- Molecular Weight:306.82
10026-12-7
119 suppliers
$15.00/10gm
61247-57-2
38 suppliers
$100.00/5g
Yield:61247-57-2 77%
Reaction Conditions:
with THF;Na#Hg in acetonitrile;NbCl5 in acetonitrile was added to Na-Hg-amalgam and acetonitrile, the mixt. was stirred for 4 h with periodic shaking, the soln. was filtered, the solvent was removed in vac., the solid was cooled to 0°C, THF was added; the mixt was stirred, allowed to come to room temp., after 4 h the soln. was filtered;
References:
Boyd, Peter D. W.;Nielsen, Alastair J.;Rickard, Clifton E. F. [Journal of the Chemical Society, Dalton Transactions,1987,p. 307 - 314]
109-99-9
1085 suppliers
$9.00/5ml
10026-12-7
119 suppliers
$15.00/10gm
61247-57-2
38 suppliers
$100.00/5g