TETRAHYDROCORTISONE 3-(B-D-*GLUCURONIDE) synthesis
- Product Name:TETRAHYDROCORTISONE 3-(B-D-*GLUCURONIDE)
- CAS Number:26312-91-4
- Molecular formula:C27H40O11
- Molecular Weight:540.6
50-03-3
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Yield:-
Steps:
Multi-step reaction with 7 steps
1: 7.4 g / H2 / palladium on calcium carbonate / pyridine / 12 h
2: 1.7 g / H2 / Raney nickel (W-2) / dioxane / 10 h
3: 390 mg / imidazole / pyridine; dimethylformamide / 1 h / Ambient temperature
4: 400 mg / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature
5: 380 mg / 30 percent H2SO4 / acetone / 0.5 h / Ambient temperature
6: 400 mg / Ag2CO3 / toluene / 12 h / Ambient temperature
7: 110 mg / 2 percent KOH / Ambient temperature; 1.) KOH/MeOH; 2h 2.) 80percent pyruvic acid, AcOH, CHCl3; 12h
References:
Hosoda;Saito;Ito;et al. [Chemical and Pharmaceutical Bulletin,1982,vol. 30,# 6,p. 2110 - 2118]
64313-94-6
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4004-80-2
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17736-20-8
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![(3α,5β,11β)-21-(Acetyloxy)-3-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-11,17-dihydroxy-pregnan-20-one](/CAS/GIF/83274-68-4.gif)
83274-68-4
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