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3783-65-1

Thiophene, 2-(2-phenylethenyl)- synthesis

13synthesis methods
-

Yield:3783-65-1 92%

Reaction Conditions:

with 2-chloroanthracene-9,10-dione;cobalt(II) diacetate tetrahydrate;butane-2,3-dione dioxime in 1,2-dichloro-ethane at 20 - 30; for 36 h;Irradiation;Schlenk technique;Sealed tube;Inert atmosphere;

References:

Zhou, Min-Jie;Zhang, Lei;Liu, Guixia;Xu, Chen;Huang, Zheng [Journal of the American Chemical Society,2021,vol. 143,# 40,p. 16470 - 16485] Location in patent:supporting information