Thiourea, N-[3-(dimethylamino)propyl]-N'-phenyl- synthesis
- Product Name:Thiourea, N-[3-(dimethylamino)propyl]-N'-phenyl-
- CAS Number:722-04-3
- Molecular formula:C12H19N3S
- Molecular Weight:237.36
Yield:722-04-3 85%
Reaction Conditions:
in dichloromethane at 20;
Steps:
2.1 Example 2
(1) Add 1mmol C in a 100ml round bottom flask,Add 10mL of dichloromethane to it, stir to dissolve,Then add 1mmol phenyl isothiocyanate, stir and react overnight at room temperature,The dichloromethane was removed by suction, and the residue obtained was settled several times with ether to remove impurities.Quality, dry, and obtain D with a yield of 85%.
References:
CN112812045,2021,A Location in patent:Paragraph 0049-0051
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