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ChemicalBook CAS DataBase List trans-Bis(triphenylphosphine)palladium dichloride

trans-Bis(triphenylphosphine)palladium dichloride synthesis

5synthesis methods
-

Yield: 99%

Reaction Conditions:

with diethylamine in tetrahydrofuranbyproducts: P(C6H5)3, 1,3-butadiene; Ar, stirred for 24 h at room temp.; volatiles removed, ppt. washed (acetone), solvent removed; NMR;

References:

Hiwatari, Kozo;Kayaki, Yoshihito;Okita, Koshi;Ukai, Tomohiro;Shimizu, Isao;Yamamoto, Akio [Bulletin of the Chemical Society of Japan,2004,vol. 77,# 12,p. 2237 - 2250]