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ChemicalBook CAS DataBase List Triallate
2303-17-5

Triallate synthesis

1synthesis methods
The production of tri-allate involves synthesising its active compound, S-(2,3,3-trichloroprop-2-en-1-yl) di(propan-2-yl)carbamothioate. This process typically starts with the preparation of the trichloropropene intermediate, followed by its reaction with diisopropylthiocarbamate to form the final molecule. The synthesis requires careful control of reaction conditions to ensure the correct thiocarbamate linkage and high purity.
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Yield:-

Reaction Conditions:

with sodium hydroxide;tetrabutylammomium bromide1.) water, 0-5 deg C, 30 min, 2.) toluene, 20-30 deg C, 2-3 h;Yield given. Multistep reaction;

References:

Chin-Hsien, Wang [Synthesis,1981,# 8,p. 622 - 623]

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