Tris(4-pyridyl)phosphine synthesis
- Product Name:Tris(4-pyridyl)phosphine
- CAS Number:94345-03-6
- Molecular formula:C15H12N3P
- Molecular Weight:265.25
1120-87-2
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94345-03-6
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Yield:94345-03-6 19%
Reaction Conditions:
Stage #1: 4-bromopyridinwith n-butyllithium;N,N,N,N,-tetramethylethylenediamine in tetrahydrofuran;diethyl ether;hexane;pentane at -115; for 0.25 h;Inert atmosphere;Schlenk technique;
Stage #2: with phosphorus trichloride in tetrahydrofuran;diethyl ether;hexane;pentane at -115 - 20;Inert atmosphere;Schlenk technique;
References:
Nurttila, Sandra S.;Brenner, Wolfgang;Mosquera, Jesús;van Vliet, Kaj M.;Nitschke, Jonathan R.;Reek, Joost N. H. [Chemistry - A European Journal,2019,vol. 25,# 2,p. 609 - 620] Location in patent:supporting information
15854-87-2
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$6.00/1g
94345-03-6
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