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ChemicalBook CAS DataBase List VINYLDIPHENYLMETHYLSILANE

VINYLDIPHENYLMETHYLSILANE synthesis

5synthesis methods
-

Yield:13107-13-6 89%

Reaction Conditions:

Stage #1: methyl magnesium iodidewith manganese(ll) chloride in tetrahydrofuran;Metallation;
Stage #2: (dibromomethyl)methyldiphenylsilane in tetrahydrofuran at 25; for 2 h;Substitution;

References:

Kakiya;Shinokubo;Oshima [Bulletin of the Chemical Society of Japan,2000,vol. 73,# 9,p. 2139 - 2147]