Z-BETA-GLU(OTBU)-OH synthesis
- Product Name:Z-BETA-GLU(OTBU)-OH
- CAS Number:83436-45-7
- Molecular formula:C17H23NO6
- Molecular Weight:337.37
![L-Aspartic acid, N-[(phenylmethoxy)carbonyl]-, 1-anhydride with 2-methylpropyl hydrogen carbonate, 4-(1,1-dimethylethyl) ester (9CI)](/CAS/20240320/GIF/41446-22-4.gif)
41446-22-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: tetrahydrofuran; diethyl ether
2: Et3N; C6H5CO2Ag
3: 89 percent / aq. LiOH / tetrahydrofuran / 1.5 h / 0 - 20 °C
References:
Raju;Mortell, Kathleen;Anandan, Sampathkumar;O'Dowd, Hardwin;Gao, Hongwu;Gomez, Marcela;Hackbarth, Corinne;Wu, Charlotte;Wang, Wen;Yuan, Zhengyu;White, Richard;Trias, Joaquim;Patel, Dinesh V. [Bioorganic and Medicinal Chemistry Letters,2003,vol. 13,# 14,p. 2413 - 2418]
![Pentanedioic acid, 3-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl methyl ester, (3R)- (9CI)](/CAS/20210111/GIF/83436-44-6.gif)
83436-44-6
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![Pentanoic acid, 5-diazo-4-oxo-3-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (3S)-](/CAS/20211123/GIF/118248-02-5.gif)
118248-02-5
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5545-52-8
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$11.19/1G
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![Pentanedioic acid, 3-[[(phenylmethoxy)carbonyl]amino]-, 1-methyl ester, (3S)-](/CAS/20210111/GIF/77856-52-1.gif)
77856-52-1
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83436-45-7
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