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1-Adamantanol

1-Adamantanol Suppliers list
Company Name:SICHUAN ZHONGBANG TECHNICAL DEVELOPING LIMITED COMPANY  Gold
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1-Adamantanol Basic information
Outline Uses
Product Name:1-Adamantanol
Synonyms:TRICYCLO[3.3.1.1(3,7)]DECAN-1-OL;TRICYCLO[3.3.1.1]DECAN-1-OL;1-Adamantol;1-Adamatanol;-Adamantyl alcohol;damantol-(1);tricyclo(3.3.1.1(sup3,7))decan-1-ol;1-HYDROXYDIAMANTANE
CAS:768-95-6
MF:C10H16O
MW:152.23
EINECS:212-202-8
Product Categories:Pharmaceutical Raw Materials;Adamantane Derivative;FINE Chemical & INTERMEDIATES;Adamantane derivatives;Adamantanes;Alcohols;Building Blocks;C9 to C10;Chemical Synthesis;Organic Building Blocks;Oxygen Compounds
Mol File:768-95-6.mol
1-Adamantanol Structure
1-Adamantanol Chemical Properties
mp 247 °C (subl.)(lit.)
Fp 240°C
storage temp. 2-8°C
Sublimation 240 ºC
BRN 1903952
CAS DataBase Reference768-95-6(CAS DataBase Reference)
NIST Chemistry Reference1-Adamantanol(768-95-6)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 22-24/25-36-26
WGK Germany 3
RTECS AU4980000
Hazard Note Irritant
HS Code 29061900
MSDS Information
ProviderLanguage
1-Hydroxyadamantane English
ACROS English
SigmaAldrich English
ALFA English
1-Adamantanol Usage And Synthesis
Outline1-adamantanol is also known as 1- hydroxide adamantane, 1-tricyclo [3.3.1.1 (3.7)] decyl alcohol. At room temperature, it is white crystalline powder with the melting point higher than 240 ℃. It is soluble in organic solvents and insoluble in water with sublimation property. It can be used for the manufacture of synthetic adamantane derivatives and adapalene. It can react with vinylidene chloride to generate 1- adamantane acetic acid. 1-adamantyl acetate can further undergo bromination and hydrolyzed into 3-hydroxy-1-adamantyl acetate which can further react with vinylidene chloride to give 1, 3-adamantane di-acetic acid.
1-adamantanol can have Friedel-Crafts alkylation reaction acetanilide in the 98% sulfuric acid medium at room temperature for direct synthesis of 1, 3-bis (4-acetylamino-phenyl) adamantane which can undergo alkaline hydrolysis for synthesis of 1, 3 bis (4-aniline) adamantane. The synthetic route has many advantages including relative high reaction yield and easy purification, etc., therefore greatly facilitating the synthesis of 1, 3-diaryl adamantane derivatives.
The above information is edited by the Chemicalbook of Dai Xiongfeng.
Uses1-adamantanol can be used as the intermediate for synthesis of adamantanes derivatives. For example, it can be used for the manufacture of synthetic adamantane derivatives and adapalene. It can react with vinylidene chloride to give 1- adamantane acetic acid.
Chemical Propertieswhite to off-white crystalline powder or needles
Tag:1-Adamantanol(768-95-6) Related Product Information
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