ChemicalBook CAS DataBase List 2-Imidazolidone

2-Imidazolidone synthesis

14synthesis methods

Product Name:2-Imidazolidone
CAS Number:120-93-4
Molecular formula:C3H6N2O
Molecular Weight:86.09

124-38-9
121 suppliers
$214.00/14L

107-15-3
9 suppliers
$11.19/25ML

120-93-4
526 suppliers
$10.00/5g

Yield:120-93-4 99%

Reaction Conditions:

with Cs₂CO₃ at 200; under 37503.8 Torr; for 2 h;Autoclave;Reagent/catalyst;Temperature;Pressure;

Steps:

1-3; 6-15 Example 1

General procedure: Example 1To 100 mL of a high-pressure stainless steel reactor equipped with a thermocouple and electric heater, 100 mmol of ethylenediamine (Aldrich Chemical) and 20 mL of 2-pyrrolidone (Aldrich Chemical) as a solvent were added, followed by carbon dioxide (CO2). , Sin Yang Gas) was washed three times.The reactor was heated to 200° C. under a carbon dioxide pressure of 1.0 MPa. At 200° C. the carbon dioxide pressure was further increased to 5.0 MPa and maintained throughout the reaction through a carbon dioxide reservoir equipped with a high pressure regulator and pressure transducer. The reaction was carried out for 2 hours, after which the reactor was cooled to room temperature and then reduced pressure to prepare urea.

References:

KR102157615,2020,B1 Location in patent:Page/Page column 10-15

201230-82-2 Synthesis