ChemicalBook--->CAS DataBase List--->13138-53-9

13138-53-9

13138-53-9 Structure

13138-53-9 Structure
IdentificationMore
[Name]

4-Nitrophthaldiamide
[CAS]

13138-53-9
[Synonyms]

1,2-BENZENEDICARBOXAMIDE,4-NITRO-
4-NITROPHTHALAMIDE
4-Nitrophthaldiamide
4-NITROPHTHALIC ACID DIAMIDE
4-nitro-2-benzenedicarboxamide
Nitrophthalamide,98%
4-Nitrophthaldiamid
4-NITROPHTHALAMIDE 99%
[EINECS(EC#)]

236-070-6
[Molecular Formula]

C8H7N3O4
[MDL Number]

MFCD00052702
[Molecular Weight]

209.16
[MOL File]

13138-53-9.mol
Chemical PropertiesBack Directory
[Melting point ]

195 °C (dec.) (lit.)
[storage temp. ]

room temp
[form ]

powder or crystals
[Appearance]

Off-white to light yellow Solid
[CAS DataBase Reference]

13138-53-9(CAS DataBase Reference)
[EPA Substance Registry System]

13138-53-9(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37/39:Wear suitable gloves and eye/face protection .
[WGK Germany ]

1
[TSCA ]

TSCA listed
Hazard InformationBack Directory
[Uses]

4-Nitrophthalamide is a stain/dye. Dyes and metabolites.
[Synthesis]

30 g (0.156 mol) 4-nitrophthalimide was stirred in 168 mL 32% ammonia solution for 24 hours. Then it was filtered, washed with cold water, and tetrahydrofuran (THF). The color of phthalimide was yellow and it turned to white as reaction proceeds. Molecular formula: C8H7N3O4. Yield: 24 g (73%). Mp: 197 ??C.
Synthesis_13138-53-9
[References]

[1] Canadian Journal of Chemistry, 1985, vol. 63, p. 121 - 128
[2] Heterocycles, 1984, vol. 22, # 9, p. 2047 - 2052
[3] Materials Research Bulletin, 2016, vol. 75, p. 144 - 154
[4] Acta Chemica Scandinavica, 1999, vol. 53, # 9, p. 714 - 720
[5] Journal of Organic Chemistry, 1990, vol. 55, # 7, p. 2155 - 2159
Spectrum DetailBack Directory
[Spectrum Detail]

4-Nitrophthaldiamide(13138-53-9)MS
4-Nitrophthaldiamide(13138-53-9)1HNMR
4-Nitrophthaldiamide(13138-53-9)13CNMR
4-Nitrophthaldiamide(13138-53-9)IR1
4-Nitrophthaldiamide(13138-53-9)IR2
4-Nitrophthaldiamide(13138-53-9)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

13138-53-9(sigmaaldrich)
[TCI AMERICA]

4-Nitrophthalamide,>98.0%(N)(13138-53-9)
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