| Identification | Back Directory | [Name]
ETHYLENE GLYCOL MONO-P-TOLYL ETHER | [CAS]
15149-10-7 | [Synonyms]
YLOTHANE
AI3-09181
p-Cresoxyethanol
Einecs 239-209-9
2-(P-TOLYLOXY)ETHANOL
Ethanol, 2-(p-tolyloxy)-
p-Methylphenyloxyethanol
2-(4-methylphenoxy)-ethano
4-(2-HYDROXYETHOXY)TOLUENE
2-(4-METHYLPHENOXY)ETHANOL
Ethanol,2-(4-methylphenoxy)-
ethyleneglycolmonotolylether
p-Cresol 2-hydroxyethyl ether
Ethanol, 2-(p-tolyloxy)- (8ci)
2-(p-Methylphenoxy)ethylalcohol
ETHYLENE GLYCOL MONO-P-TOLYL ETHER
beta-Hydroxyethyl p-methylphenyl ether
4-(2-Hydroxyethoxy)toluene
2-(4-Methylphenoxy)ethanol | [EINECS(EC#)]
239-209-9 | [Molecular Formula]
C9H12O2 | [MDL Number]
MFCD00020600 | [MOL File]
15149-10-7.mol | [Molecular Weight]
152.19 |
| Chemical Properties | Back Directory | [Melting point ]
45°C | [Boiling point ]
123°C 8mm | [density ]
1.058±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,Room Temperature | [form ]
powder to crystal | [pka]
14.30±0.10(Predicted) | [color ]
White to Almost white | [Odor]
at 100.00 %. floral jasmin animal | [Odor Type]
floral | [Cosmetics Ingredients Functions]
PERFUMING | [LogP]
1.686 (est) | [EPA Substance Registry System]
2-(4-Methylphenoxy)ethanol (15149-10-7) |
| Hazard Information | Back Directory | [Synthesis]
The general procedure for synthesizing 2-(4-methylphenoxy)ethanol from p-toluol and 2-chloroethanol was as follows: referring to Example 2 step a; the experimental operation of Example 1a was repeated using 108 g (1 mol) of p-toluol in place of p-(α,α,γ,γ-tetramethylbutyl)phenol, and mixing with 345 g (2.5 mol) of potassium carbonate powder. All other components, dosages and reaction conditions were kept unchanged, and only the addition rate of 2-chloroethanol was adjusted to 1-2 hours. Upon completion of the reaction, 2-(4-methylphenoxy)ethanol was isolated and the product was a yellow to light brown oily residue. The yield of the crude product was 88-92% and the GC purity was 90-95%. | [References]
[1] Patent: EP1892235, 2008, A1. Location in patent: Page/Page column 4
[2] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 6, p. 1557 - 1561 |
|
|