| Identification | More | [Name]
8-Quinolinecarbaldehyde | [CAS]
38707-70-9 | [Synonyms]
8-QUINOLINECARBALDEHYDE
8-QUINOLINECARBOXALDEHYDE
AKOS AUF01716
AKOS BBS-00005342
CHEMBRDG-BB 4300502
IFLAB-BB F0178-0024
ISOQUINOLINE-8-CARBALDEHYDE
ISOQUINOLINE-8-CARBOXALDEHYDE
QUINOLINE-8-CARBALDEHYDE
QUINOLINE-8-CARBOXALDEHYDE
RARECHEM AK ML 0564
RARECHEM AM LA 0004
TIMTEC-BB SBB010129
QUINOLINE-8-CARBOXALDEHYDE, 98+%
8-Quinolinecarboxaldehyde (6CI,9CI)
N-BOC-ALLYLGLYCINE
8-Quinolinecarbaldehyde ,97% | [Molecular Formula]
C10H7NO | [MDL Number]
MFCD06227440 | [Molecular Weight]
157.17 | [MOL File]
38707-70-9.mol |
| Chemical Properties | Back Directory | [Melting point ]
95-96°C | [Boiling point ]
314.3±15.0 °C(Predicted) | [density ]
1.223±0.06 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Sealed in dry,Room Temperature | [form ]
powder to crystal | [pka]
3.45±0.17(Predicted) | [color ]
Light orange to Yellow to Green | [Water Solubility ]
Insoluble in water. | [Sensitive ]
Air Sensitive | [Detection Methods]
HPLC | [BRN ]
113039 | [InChI]
InChI=1S/C10H7NO/c12-7-9-4-1-3-8-5-2-6-11-10(8)9/h1-7H | [InChIKey]
OVZQVGZERAFSPI-UHFFFAOYSA-N | [SMILES]
N1C2C(=CC=CC=2C=O)C=CC=1 | [CAS DataBase Reference]
38707-70-9(CAS DataBase Reference) | [Storage Precautions]
Air sensitive |
| Safety Data | Back Directory | [Symbol(GHS) ]
GHS07 | [Signal word ]
Warning | [Hazard statements ]
H315-H319-H335 | [Precautionary statements ]
P261-P280a-P304+P340-P305+P351+P338-P405-P501a | [Hazard Codes ]
Xi | [Risk Statements ]
R36/37/38:Irritating to eyes, respiratory system and skin .
R36/38:Irritating to eyes and skin . | [Safety Statements ]
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37/39:Wear suitable gloves and eye/face protection . | [Hazard Note ]
Irritant | [HazardClass ]
IRRITANT | [HS Code ]
29334900 |
| Hazard Information | Back Directory | [Chemical Properties]
Off-white solid | [Uses]
Quinoline-8-carboxaldehyde is an important raw material and intermediate used in organic synthesis, pharmaceuticals agrochemicals and dyestuff fields. | [Synthesis]
General method: 8-quinoline methanol was dissolved in anhydrous DMSO (10 v/v), 1 equivalent of polymer bromide was added, and the reaction mixture was stirred at room temperature for the indicated time (see Table 1). Upon completion of the reaction, the mixture was filtered and the polymer bed was washed with DMSO. The DMSO layers were combined and the reaction was quenched with an ice-water mixture and subsequently extracted with ether. The ether layer was washed sequentially with water and brine, dried over anhydrous sodium sulfate and concentrated to give pure 8-quinolinecarboxaldehyde. All products were structurally confirmed by nuclear magnetic resonance (NMR) and mass spectrometry (MS). | [References]
[1] Tetrahedron Letters, 2011, vol. 52, # 51, p. 6971 - 6973
[2] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 10, p. 3480 - 3484
[3] Angewandte Chemie - International Edition, 2016, vol. 55, # 31, p. 9084 - 9087
[4] Angew. Chem., 2016, vol. 128, # 31, p. 9230 - 9233,4 |
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