| Identification | More | [Name]
4-Methoxypiperidine | [CAS]
4045-24-3 | [Synonyms]
4-METHOXY-PIPERIDINE
4-MethoxyPiperazine
4-METHOXY-PIPERIDINE >98%
4-METHOXYPHENYLPHOSPHONICACID | [EINECS(EC#)]
223-742-9 | [Molecular Formula]
C6H13NO | [MDL Number]
MFCD06800959 | [Molecular Weight]
115.17 | [MOL File]
4045-24-3.mol |
| Chemical Properties | Back Directory | [Appearance]
Clear colorless liquid | [Boiling point ]
44°C/6.8mm | [density ]
0.93 | [storage temp. ]
Keep in dark place,Sealed in dry,2-8°C | [form ]
Liquid | [pka]
9.83±0.10(Predicted) | [color ]
Clear | [InChI]
InChI=1S/C6H13NO/c1-8-6-2-4-7-5-3-6/h6-7H,2-5H2,1H3 | [InChIKey]
ZEYSHALLPAKUHG-UHFFFAOYSA-N | [SMILES]
N1CCC(OC)CC1 | [CAS DataBase Reference]
4045-24-3(CAS DataBase Reference) |
| Hazard Information | Back Directory | [Chemical Properties]
Clear colorless liquid | [Synthesis]
The general procedure for the synthesis of 4-methoxypiperidine from the compound (CAS: 553672-12-1) was as follows: the compound (620 mg) obtained in step (1) was dissolved in methanol (20 mL) and 10% palladium-carbon catalyst (80 mg) was added. The reaction mixture was stirred for 3 hours at room temperature and under hydrogen atmosphere. Upon completion of the reaction, the reaction mixture was filtered through a membrane filter and the filtrate was concentrated under vacuum to afford 4-methoxypiperidine (290 mg, yield: 100%) as a light yellow oil. Mass spectrometry analysis (APCI) showed m/z: 116 [M + H]+. | [References]
[1] Patent: WO2007/46550, 2007, A1. Location in patent: Page/Page column 116-117 |
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J & K SCIENTIFIC LTD.
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Energy Chemical
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Jia Xing Isenchem Co.,Ltd
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