| Identification | More | [Name]
4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE | [CAS]
4246-51-9 | [Synonyms]
1,13-DIAMINO-4,7,10-TRIOXATRIDECANE 3,3'-OXYBIS(ETHYLENE-OXY)BIS(PROPYLAMINE) 4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE ALPHA, OMEGA,-BIS-(3-AMINOPROPYL)-DIETHYLENEGLYCOL ETHER BIS[2-(3-AMINOPROPOXY)ETHYL] ETHER DCA 221 DIETHYLENE GLYCOL BIS(3-AMINOPROPYL) ETHER O,O'-BIS(3-AMINOPROPYL)DIETHYLENE GLYCOL POLYGLYCOLDIAMINE 3,3’-(oxybis(2,1-ethanediyloxy))bis-1-propanamin 3,3’-(oxybis(ethyleneoxy))bis-1-propylamin 3,3’-[oxybis(2,1-ethanediyloxy)]bis-1-propanamin 3,3’-[oxybis(2,1-ethanediyloxy)]bis-1-Propanamine di(3-aminopropyl)etherofdiethyleneglycol diethyleneglycol,di(3-aminopropyl)ether q19262 di(3-aminopropyl)digol Polyglycoldiamine (DCA 221) 4,7,10-Trioxatridecane-1,13-diamine 1-Propanamine, 3,3-oxybis(2,1-ethanediyloxy)bis- | [EINECS(EC#)]
224-207-2 | [Molecular Formula]
C10H24N2O3 | [MDL Number]
MFCD00059850 | [Molecular Weight]
220.31 | [MOL File]
4246-51-9.mol |
| Questions And Answer | Back Directory | [Synthesis]

8.5 g of Raney nickel powder was added to 20 mL of a methanol solution (21.8 mmol) of ether dinitrile (20 mL), followed by the addition of 46.5 mmol of NaBH4 and 40 mL of an 8 M NaOH aqueous solution. The resulting reaction mixture was stirred for 2.5 h, maintaining the reaction temperature in a water bath between 15 and 25 °C. H2 bubbles were generated during stirring. The reaction was stopped 5 min after the bubbling ceased, and the catalyst was filtered. The reaction mixture was washed with MeOH (50 mL × 2), and the washes were combined with the mother liquor. The mixture was concentrated under vacuum, and solid KOH (19 g) was added to the residue. The diamine product salted out as a pale yellow oil. The crude product was separated and purified by vacuum distillation to obtain the target product molecule, 4,7,10-TRIOXA-1,13-TRIDECANEDIAMINE. |
| Chemical Properties | Back Directory | [Appearance]
clear colorless to light yellow liquid | [Melting point ]
-32 °C | [Boiling point ]
146-148 °C/4 mmHg (lit.) | [density ]
1.005 g/mL at 25 °C(lit.)
| [vapor pressure ]
<0.001 hPa (20 °C) | [refractive index ]
n20/D 1.464(lit.)
| [Fp ]
>230 °F
| [storage temp. ]
Store below +30°C. | [form ]
clear liquid | [pka]
10.00±0.10(Predicted) | [color ]
Colorless to Light yellow | [PH]
>12 (100g/l, H2O, 20℃) | [explosive limit]
1.1-4.5%(V) | [BRN ]
1760709 | [Cosmetics Ingredients Functions]
HAIR CONDITIONING | [InChI]
1S/C10H24N2O3/c11-3-1-5-13-7-9-15-10-8-14-6-2-4-12/h1-12H2 | [InChIKey]
JCEZOHLWDIONSP-UHFFFAOYSA-N | [SMILES]
NCCCOCCOCCOCCCN | [LogP]
-1.25 at 25℃ | [CAS DataBase Reference]
4246-51-9(CAS DataBase Reference) | [EPA Substance Registry System]
1-Propanamine, 3,3'-[oxybis(2,1-ethanediyloxy)]bis- (4246-51-9) |
| Safety Data | Back Directory | [Symbol(GHS) ]
 GHS05 | [Signal word ]
Danger | [Hazard statements ]
H290-H314-H412 | [Precautionary statements ]
P234-P273-P280-P301+P330+P331-P303+P361+P353-P305+P351+P338 | [Hazard Codes ]
C | [Risk Statements ]
R34:Causes burns. | [Safety Statements ]
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice . S36/37/39:Wear suitable protective clothing, gloves and eye/face protection . S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) . | [RIDADR ]
UN 2735 8/PG 3
| [WGK Germany ]
2
| [RTECS ]
ID6475000
| [F ]
10-34 | [Autoignition Temperature]
260 °C | [TSCA ]
TSCA listed | [REACH Registrations]
Active | [HazardClass ]
8 | [PackingGroup ]
III | [HS Code ]
29221990 | [Storage Class]
8A - Combustible corrosive hazardous materials | [Hazard Classifications]
Aquatic Chronic 3 Eye Dam. 1 Met. Corr. 1 Skin Corr. 1B | [Toxicity]
LD50 orally in Rabbit: 3160 mg/kg LD50 dermal Rabbit 2500 mg/kg |
| Hazard Information | Back Directory | [Chemical Properties]
clear colorless to light yellow liquid | [Uses]
3,3’-[Oxybis(2,1-ethanediyloxy)]bis[1-propanamine] is a passivation ligand used to enhance the water solubility and luminescence of carbon dots. | [General Description]
4,7,10-Trioxa-1,13-tridecanediamine can be used as a surface passivation agent for the synthesis of photoluminescent carbon nanodots for semiconductor applications. | [Flammability and Explosibility]
Nonflammable | [IC 50]
PEGs |
|
| Company Name: |
J & K SCIENTIFIC LTD.
|
| Telephone: |
18210857532 18210857532 |
| Website: |
https://www.jkchemical.com |
| Company Name: |
Energy Chemical
|
| Telephone: |
400-0056266 |
| Website: |
www.energy-chemical.com |
| Company Name: |
Maya High Purity Chemicals
|
| Telephone: |
+86 (573) 82222445 (0)18006601000 452520369 |
| Website: |
www.chemicalbook.com/ShowSupplierProductsList15221/0_EN.htm |
|