ChemicalBook--->CAS DataBase List--->4466-59-5

4466-59-5

4466-59-5 Structure

4466-59-5 Structure
IdentificationMore
[Name]

3,6-Dichlorophthalic anhydride
[CAS]

4466-59-5
[Synonyms]

3,6-DICHLOROPHTHALIC ANHYDRIDE
1,3-Isobenzofurandione, 4,7-dichloro-
4,7-dichloroisobenzofuran-1,3-dione
3,6-DICHLOROPHTHALIC ANHYDRIDE---WHITE POWDER, 98%---
4,7-Dichloro-1,3-isobenzofurandione
[EINECS(EC#)]

224-733-2
[Molecular Formula]

C8H2Cl2O3
[MDL Number]

MFCD00042786
[Molecular Weight]

217.01
[MOL File]

4466-59-5.mol
Chemical PropertiesBack Directory
[Appearance]

off-white to white powder
[Melting point ]

188-190 °C(lit.)
[Boiling point ]

339.1°C (rough estimate)
[density ]

1.5974 (estimate)
[storage temp. ]

under inert gas (nitrogen or Argon) at 2-8°C
[BRN ]

164697
[CAS DataBase Reference]

4466-59-5(CAS DataBase Reference)
[NIST Chemistry Reference]

3,6-Dichloro-phthalic anhydride(4466-59-5)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[F ]

10-21
Hazard InformationBack Directory
[Chemical Properties]

off-white to white powder
[Purification Methods]

Boil the anhydride in xylene (allowing any vapours which would contain H2O to be removed, e.g. Dean and Stark trap), which causes any acid present to dehydrate to the anhydride, and cool. Recrystallise it from xylene [Villiger Chem Ber 42 3539 1909, Fedoorow Izv Akad Nauk SSSR Otd Khim Nauk 397 1948, Chem Abstr 1585 1948]. [Beilstein 17/11 V 260.]
Spectrum DetailBack Directory
[Spectrum Detail]

3,6-Dichlorophthalic anhydride(4466-59-5)1HNMR
3,6-Dichlorophthalic anhydride(4466-59-5)IR
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

4466-59-5(sigmaaldrich)
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