| Identification | More | [Name]
1-(2-METHOXYPHENYL)ETHANOL | [CAS]
7417-18-7 | [Synonyms]
2-(2-Methoxyphenyl)
2-methoxy-benzeneethano
2-(ortho-anisyl) ethanol
2-(2-Hydroxyethyl)anisole
Benzeneethanol, 2-Methoxy-
2-(2-METHOXYPHENYL)ETHANOL
2-METHOXYPHENETHYL ALCOHOL
1-(2-METHOXYPHENYL)ETHANOL
Phenethyl alcohol, o-methoxy-
2-(2-methoxyphenyl)ethan-1-ol
2-Methoxyphenethyl Alcohol >
2-Methoxyphenethyl alcohol 99%
2-METHOXYPHENYL METHYL CARBINOL
ALPHA-METHYL-2-METHOXYBENZYL ALCOHOL
DL-2-METHOXY-ALPHA-METHYLBENZYL ALCOHOL | [EINECS(EC#)]
231-029-9 | [Molecular Formula]
C9H12O2 | [MDL Number]
MFCD00004512 | [Molecular Weight]
152.19 | [MOL File]
7417-18-7.mol |
| Chemical Properties | Back Directory | [Melting point ]
37 °C | [Boiling point ]
133-135 °C/10 mmHg (lit.) | [density ]
1.076 g/mL at 25 °C(lit.)
| [refractive index ]
n20/D 1.54(lit.)
| [Fp ]
>230 °F
| [storage temp. ]
Keep in dark place,Sealed in dry,Room Temperature | [form ]
clear liquid | [pka]
14.89±0.10(Predicted) | [color ]
Colorless to Light yellow | [InChI]
InChI=1S/C9H12O2/c1-11-9-5-3-2-4-8(9)6-7-10/h2-5,10H,6-7H2,1H3 | [InChIKey]
XLDRDNQLEMMNNH-UHFFFAOYSA-N | [SMILES]
C1(CCO)=CC=CC=C1OC | [LogP]
1.557 (est) | [CAS DataBase Reference]
7417-18-7(CAS DataBase Reference) |
| Hazard Information | Back Directory | [Uses]
2-Methoxyphenethyl alcohol may be used in chemical synthesis. | [Synthesis]
Step A: To a stirred suspension of 2-(2-hydroxyethyl)phenol (5 g, 36.2 mmol) and cesium carbonate (Cs2CO3, 38.9 g, 108.7 mmol) in acetone (100 mL) was slowly added iodomethane (6.2 g, 43.4 mmol) under ice-bath conditions. The reaction mixture was stirred continuously at 0 °C for 50 min. Upon completion of the reaction, the mixture was filtered to remove insoluble salts and the filtrate was concentrated under reduced pressure by rotary evaporator. The concentrated crude product was subjected to liquid-liquid extraction with ethyl acetate (EtOAc) and water. The organic layer was separated and dried with anhydrous sodium sulfate (Na2SO4), and the dried organic layer was concentrated by filtration to give 2-(2-methoxyphenyl)ethanol (4.5 g, 29.6 mmol, 82% yield) as a yellow solid. | [References]
[1] Patent: WO2015/142903, 2015, A2. Location in patent: Page/Page column 96
[2] Patent: WO2015/140133, 2015, A1. Location in patent: Page/Page column 108
[3] Patent: WO2003/103653, 2003, A1. Location in patent: Page 184-185 |
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Energy Chemical
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www.energy-chemical.com |
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T&W GROUP
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