| Identification | More | [Name]
1-(DIPHENYLMETHYL)-3-HYDROXYAZETIDINE HYDROCHLORIDE | [CAS]
90604-02-7 | [Synonyms]
1-BENZHYDRYL AZETIDIN-3-OL HCL
1-BENZHYDRYLAZETIDIN-3-OL HYDROCHLORIDE
1-(DIPHENYLMETHYL)-3-HYDROXYAZETIDINE HYDROCHLORIDE
N-BENZHYDRYLAZETIDIN-3-OL HCL
1-(Diphenylmethyl)-3-azetidinolhydrochloride
1-Benzhydrylazetidin-3-ol hydrochloride 95%
N-Benzhydrylazetidin-3-ol hydrochloride
1-Benzhydryl-3-azetidinol hydrochloride, 95%
1-(diphenylmethyl)azetidin-3-ol hydrochloride
1-benzhydryl azetindin-3-ol hydrochloride
3-azetidinol, 1-(diphenylmethyl)- | [Molecular Formula]
C16H18ClNO | [MDL Number]
MFCD00209447 | [Molecular Weight]
275.77 | [MOL File]
90604-02-7.mol |
| Safety Data | Back Directory | [Hazard Codes ]
Xi | [Risk Statements ]
R36/37/38:Irritating to eyes, respiratory system and skin . | [Safety Statements ]
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37:Wear suitable gloves . | [Hazard Note ]
Irritant | [HS Code ]
2934999090 |
| Hazard Information | Back Directory | [Uses]
1-(Diphenylmethyl)-3-Hydroxyazetidine Hydrochloride is a vital compound and can be used to synthesise 1-Benzhydrylazetidin-3-one and 1-benzhydrylazetidin-3-ol.
| [Synthesis]
General procedure for the synthesis of 1-(diphenylmethyl)-3-hydroxyazetidine hydrochloride from 1-diphenylmethyl-3-hydroxyazetidine: 1-(diphenylmethyl)-3-hydroxyazetidine (9.70 g) was suspended in a 4.5 M hydrochloric acid solution of ethyl acetate (35 mL) at room temperature and the reaction was stirred for 10 minutes. Subsequently, the solvent was removed by evaporation to give 1-(diphenylmethyl)-3-hydroxyazetidine hydrochloride (12.0 g, 100% yield). The product was characterized by 1H-NMR (300 MHz, DMSO-d6, with TMS as internal standard) with the following chemical shifts (ppm): δ 7.30-7.70 (10H, m, arylhydrogen), 5.85 (1H, s, CH), 5.80 (1H, d, OH), 4.46 (1H, m, CH), 3.70-4.20 (4H, m, CH2 ). | [References]
[1] Patent: WO2007/118830, 2007, A1. Location in patent: Page/Page column 91 |
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