Methyl 5-chloro-2-iodobenzoate
- CAS No.
- 289039-82-3
- Chemical Name:
- Methyl 5-chloro-2-iodobenzoate
- Synonyms
- Methyl 5-chloro-2-iodobenzoate;5-chloro-2-iodo-Benzoic acid Methyl ester;Benzoic acid, 5-chloro-2-iodo-, methyl ester;5-chloro-2-iodo-Benzoic acid methyl ester (9CI ACI);Benzoic acid, 5-chloro-2-iodo-, methyl ester (9CI, ACI)
- CBNumber:
- CB0245065
- Molecular Formula:
- C8H6ClIO2
- Molecular Weight:
- 296.49
- MDL Number:
- MFCD00144772
- MOL File:
- 289039-82-3.mol
- MSDS File:
- SDS
| Boiling point | 295.6±20.0 °C(Predicted) |
|---|---|
| Density | 1.837±0.06 g/cm3(Predicted) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| Appearance | Light yellow to yellow Solid |
| InChI | InChI=1S/C8H6ClIO2/c1-12-8(11)6-4-5(9)2-3-7(6)10/h2-4H,1H3 |
| InChIKey | LNCNRPALSKTJBG-UHFFFAOYSA-N |
| SMILES | C(OC)(=O)C1=CC(Cl)=CC=C1I |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |    GHS07,GHS08,GHS09 |
|---|---|
| Signal word | Warning |
| Hazard statements | H320-H351-H336-H410 |
| Precautionary statements | P501-P261-P273-P202-P201-P271-P264-P280-P391-P308+P313-P337+P313-P305+P351+P338-P304+P340+P312-P403+P233-P405 |
Methyl 5-chloro-2-iodobenzoate price More Price(35)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS110002 | Methyl 5-chloro-2-iodobenzoate 95% | 289039-82-3 | 5g | $33 | 2026-06-04 | Buy |
| Activate Scientific | AS110002 | Methyl 5-chloro-2-iodobenzoate 95% | 289039-82-3 | 25g | $141 | 2026-06-04 | Buy |
| Synthonix | M48183 | Methyl 5-chloro-2-iodobenzoate 95+% | 289039-82-3 | 100mg | $16 | 2026-05-06 | Buy |
| Synthonix | M48183 | Methyl 5-chloro-2-iodobenzoate 95+% | 289039-82-3 | 250mg | $20 | 2026-05-06 | Buy |
| Synthonix | M48183 | Methyl 5-chloro-2-iodobenzoate 95+% | 289039-82-3 | 1g | $22 | 2026-05-06 | Buy |
Methyl 5-chloro-2-iodobenzoate Chemical Properties, Uses, Production
Synthesis
67-56-1
13421-00-6
289039-82-3
General procedure for the synthesis of methyl 5-chloro-2-iodobenzoate from methanol and 5-chloro-2-iodobenzoic acid: a mixture of 5-chloro-2-iodobenzoic acid (3.0 g, 10.62 mmol), dichlorosulfoxide (12 mL), and N,N-dimethylformamide (0.6 mL) was gently heated with a heat gun until a homogeneous solution was formed (about 15 minutes). Subsequently, the reaction solution was continued to be stirred at 23 °C for 30 min, after which the solvent was removed by concentration under reduced pressure. Methanol (24 mL) was added to the crude product and stirred at 23 °C for 30 min. After the reaction was completed, the reaction solution was again concentrated under reduced pressure. The crude product was purified by rapid chromatography on a Biotage silica gel column with a gradient of cyclohexane to cyclohexane:ethyl acetate (85:15) as eluent to give methyl 5-chloro-2-iodobenzoate (3.02 g, 10.20 mmol, 96% yield).UPLC-MS analysis showed a retention time of 1.17 min and a molecular ion peak m/z 296.6 [M + H]+ , analyzed by method 12.
References
[1] Patent: WO2015/91685, 2015, A1. Location in patent: Page/Page column 69
[2] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 10, p. 2823 - 2827
[3] Angewandte Chemie - International Edition, 2013, vol. 52, # 28, p. 7177 - 7180
Methyl 5-chloro-2-iodobenzoate Preparation Products And Raw materials
Raw materials
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Preparation Products
Methyl 5-chloro-2-iodobenzoate Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Energy Chemical | 400-0056266 18918157536; | sales8178@energy-chemical.com | China | 45000 | 61 |
| Nanjing Chemlin Chemical Co., Ltd | 025-83697070 13770331960 | info@chemlin.com.cn | China | 16307 | 64 |
| CEG Chemical Science&Technology Co., Ltd. | Mobile:13665161512 | China | 1784 | 58 | |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Shanghai HuanChuan Industry Co.,Ltd. | 021-61478794 | sales@hcshhai.com | China | 9781 | 50 |
| Tianjin Jiahan Chemical Co., Ltd. | 18920613223 86-22-58055669 | sales@jiahanchem.com | China | 122 | 55 |
| Changzhou Anxuan Chemical, Co., Ltd. | 13912302692 | sales@anxuanchem.com | China | 4824 | 58 |
| Struchem Co., Ltd. | 0512-63009836 18994340901 | helen@struchem.com | China | 3966 | 60 |
| ShangHai Wisacheam Pharmaceutical Co., Ltd. | 13817485796 | tim@wisacheampharm.com | China | 3710 | 58 |
| Kaifute（Tianjin）Chemical Co., Ltd. | 022-58659859 13820733852 | sales@kftchem.com | China | 299 | 55 |
View Latest Price from Methyl 5-chloro-2-iodobenzoate manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2021-07-02 | Benzoic acid, 5-chloro-2-iodo-, Methyl ester
289039-82-3
|
$10.00-15.00 | 1KG | 99%+ HPLC | Zhuozhou Wenxi import and Export Co., Ltd |
-
- Benzoic acid, 5-chloro-2-iodo-, Methyl ester
289039-82-3
- $10.00-15.00
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
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