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DIKEGULAC DIHYDRAT

CAS No.
18467-77-1
Chemical Name:
DIKEGULAC DIHYDRAT
Synonyms
diprogulic acid;dikegulac hydrate;DIKEGULAC DIHYDRAT;DIKEGULAC DIHYDRATE;DIACETONE-2-KETOGULONICACID;Oxogulonic acid diacetonide;Diacetone-2-oxo-L-gulonic acid;2,3,4,6-DIACETONE-2-KETOGULONIC ACID;DIKEGULAC MONOHYDRATE PESTANAL 250 MG;Diprogulic acid (and its sodium salt)
CBNumber:
CB0464936
Molecular Formula:
C12H18O7
Molecular Weight:
274.27
MDL Number:
MFCD00150519
MOL File:
18467-77-1.mol
Last updated:2023-05-04 17:34:35

DIKEGULAC DIHYDRAT Properties

Melting point 88-90 °C(lit.)
Boiling point 375℃
Density 1.281
Flash point 140℃
storage temp. 2-8°C
pka 1.77±0.60(Predicted)
FDA UNII 3981541LXD
EPA Substance Registry System .alpha.-L-xylo-2-Hexulofuranosonic acid, 2,3:4,6-bis-O-(1-methylethylidene)- (18467-77-1)

SAFETY

Risk and Safety Statements

Safety Statements  22-24/25
WGK Germany  3
HS Code  29329990

DIKEGULAC DIHYDRAT price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
American Custom Chemicals Corporation PST0000462 DIKEGULAC 98.00% 18467-77-1 1G $981.75 2021-12-16 Buy
Product number Packaging Price Buy
PST0000462 1G $981.75 Buy

DIKEGULAC DIHYDRAT Chemical Properties,Uses,Production

Definition

ChEBI: Dikegulac is a member of dioxanes.

Purification Methods

Dissolve -DAG in Et2O, filter, dry (MgSO4) it, filter it again and evaporate to give a yellow oil. Addition of one drop of H2O induces crystallisation to the monohydrate, which also forms rhombic crystals on recrystallisation from 95% EtOH/H2O at room temperature. [Flatt et al. Synthesis 815 1979, Reichstein & Grussner Helv Chim Acta 17 311 1934, Takagi & Jeffrey Acta Crystallogr Sect B 34 2932 1978, cf Org Synth 55 80 1976, Beilstein 19/12 V 520.]

DIKEGULAC DIHYDRAT Preparation Products And Raw materials

Raw materials

Preparation Products

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DIKEGULAC DIHYDRAT DIKEGULAC DIHYDRATE 2,3:4,6-bis-o-(1-methylethylidene)-alpha-l-xylo-2-hexulofuranosonicaci diprogulic acid L-Diacetoneketogulonic acid monohydrate (DAKS) DIKEGULAC MONOHYDRATE PESTANAL 250 MG 2,3:4,6-di-o-isopropyliden-2-oxo-l-gulonic acid dikegulac hydrate DIACETONE-2-KETOGULONICACID Diacetone-2-oxo-L-gulonic acid 2,3,4,6-DIACETONE-2-KETOGULONIC ACID Diprogulic acid (and its sodium salt) 2,3:4,6-Diisopropylidene-2-keto-L-gulonic acid Oxogulonic acid diacetonide α-L-xylo-2-Hexulofuranosonic acid, 2,3:4,6-bis-O-(1-methylethylidene)- 18467-77-1 C12H18O7x2H2O Specialty Synthesis Monosaccharides Carbohydrate Synthesis