N-(2-Bromoethyl)phthalimide
- CAS No.
- 574-98-1
- Chemical Name:
- N-(2-Bromoethyl)phthalimide
- Synonyms
- 2-(2-Bromoethyl)isoindoline-1,3-dione;2-(2-BROMO-ETHYL)-ISOINDOLE-1,3-DIONE;AURORA KA-575;N-(2-BromoethyL;TIMTEC-BB SBB003129;N-(2-Bromoethyl)phth;SPECS AE-641/00791032;-Bromoethylphthalimide;LABOTEST-BB LT00439821;N-BROMOETHYLPHTHALIMIDE
- CBNumber:
- CB8227544
- Molecular Formula:
- C10H8BrNO2
- Molecular Weight:
- 254.08
- MDL Number:
- MFCD00005902
- MOL File:
- 574-98-1.mol
- MSDS File:
- SDS
Melting point | 80-83 °C (lit.) |
---|---|
Boiling point | 318 °C |
Density | 1.6254 (rough estimate) |
refractive index | 1.6320 (estimate) |
storage temp. | Sealed in dry,Room Temperature |
form | Crystalline Powder |
pka | -2.35±0.20(Predicted) |
color | White to slightly pink or beige |
Water Solubility | insoluble |
BRN | 148736 |
CAS DataBase Reference | 574-98-1(CAS DataBase Reference) |
NIST Chemistry Reference | N-(beta-bromoethyl)phthalimide(574-98-1) |
EPA Substance Registry System | 1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethyl)- (574-98-1) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS05 |
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Signal word | Danger | |||||||||
Hazard statements | H314-H290 | |||||||||
Precautionary statements | P501-P260-P234-P264-P280-P390-P303+P361+P353-P301+P330+P331-P363-P304+P340+P310-P305+P351+P338+P310-P406-P405 | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 24/25 | |||||||||
WGK Germany | 3 | |||||||||
TSCA | Yes | |||||||||
HS Code | 29251995 | |||||||||
NFPA 704 |
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N-(2-Bromoethyl)phthalimide price More Price(43)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich | B66302 | N-(2-Bromoethyl)phthalimide 95% | 574-98-1 | 25g | $52.8 | 2024-03-01 | Buy |
Sigma-Aldrich | B66302 | N-(2-Bromoethyl)phthalimide 95% | 574-98-1 | 100g | $57.78 | 2024-03-01 | Buy |
TCI Chemical | B0597 | N-(2-Bromoethyl)phthalimide >98.0%(GC)(T) | 574-98-1 | 25g | $48 | 2024-03-01 | Buy |
TCI Chemical | B0597 | N-(2-Bromoethyl)phthalimide >98.0%(GC)(T) | 574-98-1 | 100g | $157 | 2024-03-01 | Buy |
Alfa Aesar | A12164 | N-(2-Bromoethyl)phthalimide, 98+% | 574-98-1 | 25g | $38.65 | 2024-03-01 | Buy |
N-(2-Bromoethyl)phthalimide Chemical Properties,Uses,Production
Chemical Properties
white powder
Uses
N-(2-Bromoethyl)phthalimide is an intermediate used in organic synthesis. It can react with phenyl magnesium bromide to get 2-(2-bromo-ethyl)-3-hydroxy-3-phenyl-isoindolin-1-one.
Synthesis Reference(s)
Journal of the American Chemical Society, 71, p. 2425, 1949 DOI: 10.1021/ja01175a052
Organic Syntheses, Coll. Vol. 1, p. 119, 1941
Purification Methods
The following is to be carried out in an efficient FUME HOOD. Dissolve the compound (180g) in CS2 (500 mL) by refluxing for 15minutes (to cause the separation of the most likely impurity, 1,2-diphthalimidoethane), filter and evaporate under reduced pressure. The product forms light tan crystals (m 78-80o). Recrystallise it from EtOH (charcoal) [the compound (50g) is dissolved in hot 75% EtOH (200mL), boiled for ca 10 minutes, carbon is added (5g, Norite), filter and cool to 0o], to give white crystals (40g) which can be recrystallised (m 80-81o); and further recrystallisation gives m 82-83o. [Salzberg & Supniewski Org Synth Coll Vol I 119 1932, Landini & Rolla Synthesis 389 1976, Beilstein 21/10 V 275.]
N-(2-Bromoethyl)phthalimide Preparation Products And Raw materials
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21687 | 55 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32715 | 60 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418679 +86-18949832763 | info@tnjchem.com | China | 2989 | 55 |
Zjartschem | +86-571-8723 8903 jocelynpan@zjarts.com | jocelynpan@zjarts.com | CHINA | 993 | 58 |
Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 | sales@ansciepchem.com | CHINA | 4242 | 58 |
HaBo Hong Kong Co., Limited. | +86-25-18512596065 | info@habotech.com | CHINA | 933 | 58 |
Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28180 | 58 |
Accela ChemBio Inc. | (+1)-858-699-3322 | info@accelachem.com | United States | 19965 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49391 | 58 |
career henan chemical co | +86-0371-86658258 15093356674; | factory@coreychem.com | China | 29826 | 58 |
View Lastest Price from N-(2-Bromoethyl)phthalimide manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2023-03-06 | N-(2-Bromoethyl)phthalimide
574-98-1
|
US $10.00 / KG | 1KG | 99.8% | 100000kgs | Hebei Guanlang Biotechnology Co,.LTD | ||
2019-12-23 | N-(2-Bromoethyl)phthalimide
574-98-1
|
US $1.00 / g | 100g | 99% | G/KG/T | Career Henan Chemical Co |
- N-(2-Bromoethyl)phthalimide
574-98-1
- US $10.00 / KG
- 99.8%
- Hebei Guanlang Biotechnology Co,.LTD
- N-(2-Bromoethyl)phthalimide
574-98-1
- US $1.00 / g
- 99%
- Career Henan Chemical Co