(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE
- CAS No.
- 13726-21-1
- Chemical Name:
- (4-CHLORO-3-METHOXYPHENYL)ACETONITRILE
- Synonyms
- RARECHEM AL MP 0203;2-(4-Chloro-3-methoxyphenyl);(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE;2-(4-Chloro-3-Methoxyphenyl)acetonitrile;Benzeneacetonitrile, 4-chloro-3-methoxy-;2-(4-Chloro-3-methoxyphenyl)acetonitrilev
- CBNumber:
- CB82452470
- Molecular Formula:
- C9H8ClNO
- Molecular Weight:
- 181.62
- MDL Number:
- MFCD09907926
- MOL File:
- 13726-21-1.mol
| Product description | Number | Pack Size | Price |
| 2-(4-Chloro-3-methoxyphenyl)acetonitrile | 6563AA | 1g | $447 |
| (4-Chloro-3-methoxyphenyl)acetonitrile >97% | 116087 | 500mg | $544 |
| (4-Chloro-3-methoxyphenyl)acetonitrile >97% | 116087 | 1g | $730 |
| 4-CHLORO-3-METHOXY-BENZENEACETONITRILE 95.00% | HCH0314348 | 1G | $808.5 |
| 2-(4-chloro-3-methoxyphenyl)acetonitrile 95+% | CM132004 | 5g | $926 |
(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE price
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | 6563AA | 2-(4-Chloro-3-methoxyphenyl)acetonitrile | 13726-21-1 | 1g | $447 | 2021-12-16 | Buy |
| Matrix Scientific | 116087 | (4-Chloro-3-methoxyphenyl)acetonitrile >97% | 13726-21-1 | 500mg | $544 | 2021-12-16 | Buy |
| Matrix Scientific | 116087 | (4-Chloro-3-methoxyphenyl)acetonitrile >97% | 13726-21-1 | 1g | $730 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0314348 | 4-CHLORO-3-METHOXY-BENZENEACETONITRILE 95.00% | 13726-21-1 | 1G | $808.5 | 2021-12-16 | Buy |
| Chemenu | CM132004 | 2-(4-chloro-3-methoxyphenyl)acetonitrile 95+% | 13726-21-1 | 5g | $926 | 2021-12-16 | Buy |
(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Chemical Properties,Uses,Production
Synthesis
143-33-9
103347-14-4
13726-21-1
To a 90% ethanol (500 mL) solution of 4-(bromomethyl)-1-chloro-2-methoxybenzene (68.5 g, 0.290 mol) was added sodium cyanide (28.5 g, 0.580 mol). The reaction mixture was stirred at 60 °C overnight. Upon completion of the reaction, the ethanol was removed by evaporation under reduced pressure and the residue was dissolved in water. The aqueous phase was extracted with ethyl acetate (300 mL × 3). The organic layers were combined, washed with saturated saline, and dried over anhydrous sodium sulfate. Purification by silica gel column chromatography (eluent: petroleum ether/ethyl acetate = 30:1) afforded 4-chloro-3-methoxyphenylacetonitrile (25 g, 48% yield).1H NMR (400 MHz, CDCl3) δ 7.36 (d, J = 8 Hz, 1H), 6.88-6.84 (m, 2H), 3.92 (s, 3H), 3.74 (s, 2H ).13C NMR (100 MHz, CDCl3) δ 155.4, 130.8, 129.7, 122.4, 120.7, 117.5, 111.5, 56.2, 23.5.
References
[1] Patent: US2007/244159, 2007, A1. Location in patent: Page/Page column 91
[2] Patent: US2005/239881, 2005, A1. Location in patent: Page/Page column 27
[3] Patent: WO2007/39736, 2007, A1. Location in patent: Page/Page column 28
[4] Patent: US2008/293775, 2008, A1. Location in patent: Page/Page column 22
[5] Patent: US2004/192704, 2004, A1. Location in patent: Page 23
(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
| Changzhou Anxuan Chemical Co., Ltd | +86-0519-89882563 +86-18961279162 | andy@anxuanchem.com | China | 4327 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +8613336024896 | CB@aromsyn.com | China | 19183 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Beijing Eternalchem Co,. Ltd. | 010-59484199 18611897322 | sales@eternalchem.com | China | 4383 | 60 |
| Shanghai HuanChuan Industry Co.,Ltd. | 021-61478794 | sales@hcshhai.com | China | 9793 | 50 |
| Cool Pharm, Ltd | 021-60455363 18019463053 | sales@coolpharm.com | China | 12346 | 58 |
| Changzhou Anxuan Chemical, Co., Ltd. | 13912302692 13912302692; | sales@anxuanchem.com | China | 4828 | 58 |
| Aikon International Limited | 025-58859352 18068836627 | dt3@aikonchem.com | China | 15493 | 58 |
