2-[2-(2-Azidoethoxy)ethoxy]ethanamine
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2-[2-(2-Azidoethoxy)ethoxy]ethanamine 속성
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
HS 번호 | 2929900090 |
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신호 어: | Danger | ||||||||||||||
유해·위험 문구: |
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예방조치문구: |
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2-[2-(2-Azidoethoxy)ethoxy]ethanamine C화학적 특성, 용도, 생산
Synthesis
2-[2-(2-Hydroxyethoxy)ethoxy]ethyl chloride (15 g, 88.9 mmol), NaI(4.06 g, 27.1 mmol), and NaN3 (45.3 mg, 697 mmol) were dissolved in distilled water (90 mL), and the solution was stirred for 48 h at 50 °C. The reaction mixture extracted with ethyl acetate for three times. The organic layer was dried over Na2SO4 , and evaporated to collect 2-[2-(2-azidoethoxy)ethoxy]ethanol (14.0 g, 90.1%) as a yellow oil.To the solution 2-[2-(2-azidoethoxy)ethoxy]ethanol (8 g, 45.7 mmol) in THF (22.4 mL), 6 M NaOH(20.8 mL) and TsCl (13.1 g, 68.6 mmol) were added at 0 °C. The reaction mixture was stirred for 1 h at room temperature under nitrogen atmosphere. The solution was then extracted with diethyl ether four times, and the organic layer was washed with 1 M NaOH. After evaporation of the organic layer,2-[2-(2-azidoethoxy)ethoxy]ethyl tosylate (16.8 g, 98.6%) was obtained as a yellow oil.Finally, ammonia solution (28%, 14.8 mL, 365 mol) was added to the 2-[2-(2-azidoethoxy)ethoxy]-ethyl tosylate (8 g, 24.3 mmol) dissolved in THF (95.9 mL), and reaction mixture was stirred for 96 h at 40 °C. After the reaction, distilled water (50 mL) was added to the solution. The mixture was washed with diethyl ether and then extracted with dichloromethane. The organic layer was dried over NaSO4 and evaporated to obtain 2-[2-(2-azidoethoxy)ethoxy]ethanamine (2.49 g, 58.8%) as a yellow oil.2-[2-(2-Azidoethoxy)ethoxy]ethanamine 준비 용품 및 원자재
원자재
Ethanamine, 2-[2-(2-bromoethoxy)ethoxy]-
BOC-1-아미노-3,6-디옥사-8-옥탄디아민
트라이에틸렌 글라이콜 다이아민
에탄,1,2-비스(2-브로모에톡시)-
t-Boc-N-아미도-PEG2-아자이드
(2-[2-(2-HYDROXY-ETHOXY)-ETHOXY]-ETHYL)-카르밤산TERT-부틸에스테르
트리에틸렌글리콜디메탄술포네이트
Tri(Ethylene Glycol) DI-P-Toluenesulfonate
1,8-디아지도-3,5-디옥사옥탄
트리글리콜 디클로라이드
트라이에틸렌 글라이콜
준비 용품
2-[2-(2-Azidoethoxy)ethoxy]ethanamine 공급 업체
글로벌( 109)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
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ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32836 | 60 |
Accela ChemBio Inc. | +1-858-6993322 |
info@accelachem.com | United States | 19536 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 |
sales@chemdad.com | China | 39916 | 58 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 |
sales@conier.com | China | 49392 | 58 |
SHANGHAI T&W PHARMACEUTICAL CO., LTD. | +86-021-61551413 +8618813727289 |
contact@trustwe.com | China | 5738 | 58 |
Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 |
sale04@alfachem.cn | China | 13349 | 58 |
TargetMol Chemicals Inc. | +1-781-999-5354 +1-00000000000 |
marketing@targetmol.com | United States | 19892 | 58 |
Wuhan Borenpharm Co., Ltd | 027-65563561 18717150066 |
3207347307@qq.com | CHINA | 1238 | 58 |
Shanxi Xuanran Import and Export Trade Co., Ltd. | +8617735180244 |
mike_yan@xuanranglobal.com | CHINA | 4022 | 58 |
Nextpeptide Inc | +86-0571-81612335 +8613336028439 |
sales@nextpeptide.com | China | 19915 | 58 |
2-[2-(2-Azidoethoxy)ethoxy]ethanamine 관련 검색:
펜타에틸렌 글리콜 3-말레이미도-프록실
2-(2-Azidoethoxy)ethanol
Biotin-PEG3-propionic acid
HS-PEG4-tBu
5,8,11,14-Tetraoxa-2-azahexadecanoic acid,16-amino-,1,1-dimethyl ester
3,6,9,12-tetraoxatridecylamine
H2N-PEG4-tBu
1H-Thieno[3,4-d]imidazole-4-pentanamide,N-(14-amino-3,6,9,12-tetraoxatetradec-1-yl)hexahydro-2-oxo-,(3aS,4S,6aR)-
Decaethylene glycol
O-(2-AMINOETHYL)-O-(2-(BOC-AMINO)ETHYL)OCTAETHYLENE GLYCOL
2-[2-(2-methoxyethoxy)ethoxy]-ethanethiol
2,5,8,11,14,17,20,23-Octaoxapentacosane-25-thiol
HEPTAETHYLENE GLYCOL
FMOC-15-AMINO-4,7,10,13-TETRAOXAPENTADECANOIC ACID
MPEG7-CH2CH2COOH
(R)-N-(3,6,9,12-Tetraoxatridecyl)-alpha-lipoamide
Z-15-aMino-4,7,10,13-tetraoxapentadecacanoic acid