9- 페닐 안트라센
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9- 페닐 안트라센 속성
- 녹는점
- 153-155 °C (lit.)
- 끓는 점
- 417 °C (lit.)
- 밀도
- 1.1180 (estimate)
- 굴절률
- 1.7040 (estimate)
- 저장 조건
- Sealed in dry,Room Temperature
- 용해도
- 클로로포름(약간 용해됨), 에틸아세테이트(약간 용해됨)
- 물리적 상태
- 고체
- 물리적 상태
- 단단한 모양
- 색상
- 미색부터 옅은 갈색까지
- 감도
- Light Sensitive
- BRN
- 1910570
- CAS 데이터베이스
- 602-55-1(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
9- 페닐 안트라센 C화학적 특성, 용도, 생산
화학적 성질
Pale Yellow Plates용도
9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.제조 방법
The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.Synthesis of 9-phenylanthracene
Purification Methods
Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]9- 페닐 안트라센 준비 용품 및 원자재
원자재
준비 용품
9- 페닐 안트라센 공급 업체
글로벌( 180)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 |
xinshengkeji@xsmaterial.com | China | 1090 | 58 |
Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 |
info@spring-chem.com | China | 2068 | 57 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 |
info@dakenam.com | China | 18628 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32836 | 60 |
AB PharmaTech,LLC | 323-480-4688 |
United States | 989 | 55 | |
Beijing Green Guardee Technology Co., Ltd | 86-010-69706062 |
sales2@greenguardee.com | CHINA | 650 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 |
sales@coreychem.com | China | 29888 | 58 |
Xiamen AmoyChem Co., Ltd | +86-592-6051114 +8618959220845 |
sales@amoychem.com | China | 6387 | 58 |
BAYNOE CHEM CO.,LTD | +86-21-34783353 +8615000719740 |
baynoe@baynoe.com | CHINA | 934 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 |
sales@chemdad.com | China | 39916 | 58 |
9- 페닐 안트라센 관련 검색:
9-브로 모-10-phenylanthracene (10-Phenylanthracen-9-yl) boronic 산 9,10-디페닐안트라센 루브렌 9- 페닐 안트라센 9,10- 비스 (2- 나프 틸) 안트라 세스 9,10- 디 나프탈렌 -1- 일 안트라센 안트라센 2-클로로-9,10-디페닐안트라센 다이벤조[a,e]플루오란텐
9,10-BIS(4-METHOXYPHENYL)ANTHRACENE
FLUOROL YELLOW 088
9,10-Bis(4-methoxyphenyl)-2-chloroanthracene
2-TERTBUTYL-9,10-DI(2-NAPHTHYL)ANTHRACENE
9,10-BIS[3-METHYLPHENYL]ANTHRACENE
9,9'-Bianthracene
9,10-BIS(3,5-DIHYDROXYPHENYL)ANTHRACENE
7-METHYLBENZ[A]ANTHRACENE