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Aminoacetonitrile hydrochloride

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Products Intro: Product Name:Aminoacetonitrile hydrochloride
CAS:6011-14-9
Purity:99% Package:25KG
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Products Intro: Product Name:Aminoacetonitrile hydrochloride
CAS:6011-14-9
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CAS:6011-14-9
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CAS:6011-14-9
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Products Intro: Product Name:Aminoacetonitrile hydrochloride
CAS:6011-14-9
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Aminoacetonitrile hydrochloride manufacturers

Aminoacetonitrile hydrochloride Basic information
Product Name:Aminoacetonitrile hydrochloride
Synonyms:aminoacetonitrilemonohydrochloride;amino-acetonitrilmonohydrochloride;glycinonitrile,monohydrochloride;2-AminoacetonitrileHydrochloride;GlycinonitrileHCl;Aminoacetonitrilehydrochloride,97%;Acetonitrile, amino-, monohydrochloride;AMINOACETONITRILE A.K.A. GLYCINONITRILE HYDROCHLOR
CAS:6011-14-9
MF:C2H5ClN2
MW:92.53
EINECS:227-865-9
Product Categories:Pharmaceutical Intermediates;straight chain compounds
Mol File:6011-14-9.mol
Aminoacetonitrile hydrochloride Structure
Aminoacetonitrile hydrochloride Chemical Properties
Melting point 172-174°C
RTECS MC1950000
storage temp. Inert atmosphere,Room Temperature
solubility Methanol (Slightly, Heated), Water
form Powder
color White to Off-White
Water Solubility Soluble in water 20°C, 1000g/L.
Sensitive Hygroscopic
Merck 14,412
CAS DataBase Reference6011-14-9(CAS DataBase Reference)
EPA Substance Registry SystemAminoacetonitrile hydrochloride (6011-14-9)
Safety Information
Risk Statements 20/21/22-36/37/38-25
Safety Statements 22-36/37-45-26
RIDADR 3439
TSCA Yes
HazardClass 6.1
PackingGroup III
HS Code 29269090
MSDS Information
ProviderLanguage
Aminoacetonitrile hydrochloride English
ALFA English
Aminoacetonitrile hydrochloride Usage And Synthesis
Chemical PropertiesWhite to light brown solid
UsesUsed as pharmaceutical intermediates, organic synthetic raw material transportation.
ApplicationAminoacetonitrile is a useful synthetic intermediate. It is a reagent used to synthesize dipeptide nitriles as reversible and potent cathepsin S inhibitors. It can also used to prepare substituted cyclic ureas as possible HIV protease inhibitors.
PreparationSynthesis of Aminoacetonitrile Hydrochloride by Reaction of Aminoacetonitrile with Hydrogen Chloride in Methanol: mixing the aminoacetonitrile with hydrogen chloride methanol solution, reacting at 45-50°C for 1-2 hours, cooling to below 5°C, filtering, and centrifugalizing to obtain the aminoacetonitrile hydrochloride, wherein in the hydrogen chloride methanol solution, the content of hydrogen chloride is 30-50 wt%, and the water content is less than or equal to 1%.
Preparation method of aminoacetonitrile hydrochloride
Safety ProfileAn experimental teratogen. Experimental reproductive effects. When heated to decomposition it emits toxic fumes of NOx and HCl.
Purification MethodsThe salt recrystallises from dilute EtOH as hygroscopic leaflets. It is best to crystallise it from absolute EtOH/Et2O (1:1) and then recrystallise it from absolute EtOH. The melting point recorded ranges from 144o to 174o. The free base has b 58o/15mm with partial decomposition. [Klages J Prakt Chem [2] 65 189 1902, Mange J Am Chem Soc 56 2197 1934, Goldberg & Kelly J Chem Soc 1371 1947, Beilstein 4 H 344, 4 I 468, 4 II 783, 4 III 1120, 4 IV 2363.]
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