|
| tert-Butyl 4-(bromomethyl)benzoate Basic information |
Product Name: | tert-Butyl 4-(bromomethyl)benzoate | Synonyms: | 4-(BROMOMETHYL)-BENZOIC ACID, 1,1-DIMETHYLETHYL ESTER;TERT-BUTYL P-(BROMOMETHYL) BENZOATE;4-Bromomethyl-benzoic acid tert-butyl ester;t-butyl-4-bromomethylbenzoate;1,1-DIMETHYLETHYL 4-(BROMOMETHYL)BENZOATE;4-BROMO METHYL BENZOIC ACID MONO TERT-BUTYL ESTER;tert-Butyl 4-(bromomethyl)benzoate;4-Benzoic acid mono tert-butyl ester | CAS: | 108052-76-2 | MF: | C12H15BrO2 | MW: | 271.15 | EINECS: | 691-573-1 | Product Categories: | | Mol File: | 108052-76-2.mol | |
| tert-Butyl 4-(bromomethyl)benzoate Chemical Properties |
Melting point | 53-55 °C | Boiling point | 320.9±25.0 °C(Predicted) | density | 1.313±0.06 g/cm3(Predicted) | storage temp. | under inert gas (nitrogen or Argon) at 2-8°C | solubility | DMF: 30 mg/ml; DMSO: 30 mg/ml; Ethanol: 30 mg/ml; Ethanol:PBS (pH 7.2)(1:3): .25 mg/ml | form | A crystalline solid | CAS DataBase Reference | 108052-76-2(CAS DataBase Reference) |
| tert-Butyl 4-(bromomethyl)benzoate Usage And Synthesis |
Synthesis |
To a solution of substituted toluene in carbon tetrachloride were added N-bromosuccinimide (1.1 equiv) and 2,2'-azobis(isobutyronitrile) (0.15 equiv). The mixture was refluxed, then filtered and concentrated. The residue was purified by silica gel column chromatography to give tert-Butyl 4-(bromomethyl)benzoate.
|
| tert-Butyl 4-(bromomethyl)benzoate Preparation Products And Raw materials |
|