| Company Name: |
INTATRADE GmbH |
| Tel: |
+49 3493/605464 |
| Email: |
sales@intatrade.de |
- 4-Hydroxyphthalonitrile
-
- $209.30
-
2026-09-30
- CAS:30757-50-7
- Min. Order: 25Kg/Drum
- Purity: 98.0%Min
- Supply Ability: 3tons/month
- 4-Hydroxyphthalonitrile
-
- $281.69
-
2026-09-30
- CAS:30757-50-7
- Min. Order: 25Kg/Drum
- Purity: 98.5%min, 99.5%min
- Supply Ability: 2tons/month
|
| | 4-Hydroxyphthalonitrile Basic information |
| | 4-Hydroxyphthalonitrile Chemical Properties |
| Melting point | ~218 °C | | Boiling point | 394.6±37.0 °C(Predicted) | | density | 1.34±0.1 g/cm3(Predicted) | | storage temp. | Inert atmosphere,Room Temperature | | solubility | soluble in Methanol | | form | powder to crystal | | pka | 6.45±0.18(Predicted) | | color | White to Gray to Brown | | BRN | 2718847 | | InChIKey | FTVOPKROFUTOKY-UHFFFAOYSA-N | | CAS DataBase Reference | 30757-50-7(CAS DataBase Reference) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-36 | | WGK Germany | 3 | | HS Code | 2926907090 |
| | 4-Hydroxyphthalonitrile Usage And Synthesis |
| Chemical Properties | Colorless transparent liquid | | Synthesis Reference(s) | Synthetic Communications, 19, p. 3231, 1989 DOI: 10.1080/00397918908052723 | | Synthesis | The general procedure for the synthesis of 3,4-dicyanophenol from 4-nitrophthalonitrile was as follows: 1) 103.9 g (600 mmol) of 4-nitrophthalonitrile and 800 mL of dimethyl sulfoxide (DMSO) were added to a three-necked flask equipped with a stirrer. After the solid was completely dissolved, 91.0 g (660 mmol) of potassium carbonate and 46.0 g (660 mmol) of sodium nitrite were added sequentially. The reaction mixture was heated to 160 °C and kept at reflux for 5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently poured into a large amount of water to precipitate the product. The yellow solid was collected by filtration and dried under vacuum at 110 °C to give 73.3 g of 4-hydroxyphthalonitrile in 85% yield. | | References | [1] RSC Advances, 2015, vol. 5, # 96, p. 79207 - 79215
[2] Patent: CN104910113, 2017, B. Location in patent: Paragraph 0041-0042; 0045-0046
[3] Synthetic Communications, 1989, vol. 19, # 18, p. 3231 - 3240
[4] Russian Journal of General Chemistry, 2011, vol. 81, # 4, p. 768 - 772 |
| | 4-Hydroxyphthalonitrile Preparation Products And Raw materials |
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